EM-Tec silicon nitride support films and membranes for EM

affordable, next generation silicon nitride membranes with unique frame design

20nm silicon nitride support films   Ι   50nm silicon nitride support films   Ι   200nm silicon nitride support films

Introduction

 

The EM-Tec silicon nitride films are the next generation silicon nitride films and include improvements on previous generations of silicon nitride support films. They combine debris free, stress optimised engineered films on a novel hexagonal robust silicon frame which has a reference mark for to enable sample/frame location and flat micro-structured TrueGrip edges. The properties of silicon nitride enables to produce a strong, chemical resistant, carbon free, low background ultra-flat TEM support film. They are ideal for application such as nano particle imaging, quantitative carbon analysis, chemical experimentation on the support films, real-time chemical reactions and crystal growth research, thin film research,  on-film cell growth and multiple microscopy research techniques. The EM-Tec silicon nitride membranes are stress optimised for each window size and film thickness using proprietary algorithms and chemistry formulations. These support films are manufactured using state-of-the-art MEMS technology to produce debris-free, clean and highly planar membranes. 
The unique hexagonal shaped silicon frame has been developed to facilitate easy handling. The parallel sides together with the micro-structured TrueGrip edges enable easy pickup and handling of the frames compared to round frames or clipped silicon frames.  The reference mark on one of the side helps with the orientation when the support films goes through multiple procedures. The unique hexagonal frames have a side length of 1.52mm and are fully compatible with the standard 3mm TEM grid. The 200µm frame thickness will fit most TEM sample holders. Packaged per 10 support films in the EM-Tec #28-000100 TEM grid box.

  The aperture frames are made from silicon with a thickness of 200µm. Backside of the frame (larger opening) has a coating of 50nm silicon nitride. The unique hexagonal shaped silicon frame has been developed to facilitate easy handling
The aperture frames with their unique hexagonal shaped silicon frame
has been developed to facilitate easy pickup and handling.

 

Benefits of using silicon nitride membranes:

  • amorphous, low background, low scattering material
  • high resistance to acids, bases and solvents
  • high temperature resistant up to 1000° C
  • carbon free, easily cleaned
  • large viewing area without bars
  • ideal support for multiple microscopy techniques such as TEM, SEM, FIB, EDX, Auger, XPS and AFM/SPM

 

Features of the EM-Tec silicon nitride support films for EM:

  • sturdy silicon nitride films with 20, 50 and 200nm thickness
  • clean, debris-free silicon nitride membranes
  • optimised membrane stress to achieve strength and high planarity
  • unique hex shape frames for easy handling
  • reference mark in hex shape frame to assist with sample/frame location
  • flat, micro-structured TrueGrip edges


Specifications of the EM-Tec silicon nitride support films for EM:

Aperture size

Membrane thickness / Type*

Frame thickness

Frame shape /diameter

0.25 x 0.25mm

-

50nm / LS

200nm / ULS

200 µm

Hex 1.52mm / Ø3.05mm

0.50x0.50mm

-

50nm / ULS

200nm / ULS

200 µm

Hex 1.52mm / Ø3.05mm

1.0 x 1.0mm

-

50nm / ULS

200nm / ULS

200 µm

Hex 1.52mm / Ø3.05mm

1.5 x 0.5mm

-

50nm / ULS

200nm / ULS

200 µm

Hex 1.52mm / Ø3.05mm

2 x 1.5 x 0.1mm

20nm / LS

50nm / LS

200nm / ULS

200 µm

Hex 1.52mm / Ø3.05mm

9 x 0.1 x 0.1mm

20nm / LS

50nm / LS

200nm / ULS

200 µm

Hex 1.52mm / Ø3.05mm

* ULS = Ultra-Low Stress, LS = Low Stress

Technical Support Bulletin: TSB 23-020025 Silicon Nitride Support Films & Silicon Apertures.

  EM-Tec Silicon Nitride Support Films for EM

50nm Silicon Nitride Films

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